발간논문

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Vol.49, No.5, 367 ~ 374, 2011
Title
Synthesis and Characterization of Anatase TiO2 Powder using a Homogeneous Precipitation Method
최순옥 Soon Ok Choi , 조지희 Jee Hee Cho , 임성환 Sung Hwan Lim , 정은영 Eun Young Chung
Abstract
This paper studies the experimental method that uses the homogeneous precipitation method to prepare mica flakes coated with anatase-type titania pearlescent pigment with urea as precipitant. The optimum technology parameters, the chemical composition, the microstructure, and the color property of resulting pigments are discussed. The coating principle of mica coated titania with various coating thickness is analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy(TEM) and tested by spectrophotometer analysis. The colored nanocrystalline pigments with different morphology and coating thickness 45-170 nm were prepared by homogeneous precipitation treatment of TiOSO4(titanum oxysulfate) aqueous solutions. Characterizations on the pigments show that the pearlescent effects of the pigments depend mainly on mica size, thickness of the metal oxide deposit, its chemical composition, and crystal structure.
Key Words
titania, mica, pigments, optical property, transmission electron microscopy
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