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In order to improve the corrosion resistance of Fe-20Cr-1.7C-1Si hardfacing alloy without a loss of wear resistance, the effect of Ni addition was investigated. As expected, the corrosion resistance of the alloy increased with increasing Ni concentration. The wear resistance of the alloy did not decrease, even though the hardness decreased, up to Ni concentration of 5 wt.%. This was attributed to the fact that the decrease in hardness was counterbalanced by the strain-induced martensitic transformation. The wear resistance of the alloy, however, decreased abruptly with increases of the Ni concentration over 5 wt.%.

keyword : Alloys, Costing, Wear, X-ray diffraction, Phase transformation

In this study, the interlaminar fracture behaviors of laminated GFRP composites were investigated, and the results could be used for damage tolerance design based on fracture mechanics. Three types of laminated GFRP composites that can be used as high voltage insulating materials in magnet systems were fabricated in order to study the interlaminar fracture behavior according to the molding process. The values of interlaminar fracture toughness for the VPI, prepreg, and HPL laminate were 1.9 MPa · 1/2, 1.7 MPa · 1/2, and 2.2 MPa · 1/2, respectively. HPL laminate showed the best fracture resistance. The failure modes of HPL and VPI were similar to that of an adhesive joint, and prepreg laminates showed partial cohesive failure mode due to internal voids.

keyword : composites, fracture toughness, mechanical properties, GFRP

This paper presents a study of the tensile behavior of carbon and glass fiber reinforced epoxy hybrid laminates manufactured by vacuum assisted resin transfer molding (VARTM). The objective of this study was to develop and characterize carbon fiber reinforced plastic hybrid composite material that is low cost and light-weight and that possesses adequate strength and stiffness. The effect of position and content of the glass fabric layer on the tensile properties of the hybrid laminates was examined. The strength and stiffness of the hybrid laminates showed a steady decrease with an increase of the glass fabric content this decrease was almost linear. Fracture strain of these laminates showed a slight increasing trend when glass fabric content was increased up to 3 layers, but at a glass fabric content > 3 layers the strain was almost constant. When glass fabric layers were at both outer surfaces, the hybrid laminate exhibited a slightly higher tensile strength and elastic modulus due to the small amount of glass yarn pull-out.

keyword : composites, fracture, mechanical properties, tensile test, hybrid Laminate

In this study, three kinds of linepipe steels were processed by changing the amount of Mo and Nb to investigate the effects on microstructures, tensile and Charpy impact properties. All the specimens consisted of acicular ferrite, granular bainite and secondary phases such as martensite and austenite constituents (MA). The increase in Mo raised the volume fractions of the granular bainite and MA, and raised the number of fine precipitates, which increased the yield and tensile strengths and decreased the upper self energy and energy transition temperatures. In the steel having less Mo and more Nb, the volume fractions of the granular bainite and MA decreased, and a finer microstructure was observed. This microstructure suppressed the formation of separation during Charpy impact testing and led to a higher upper shelf energy and lower energy transition temperature, while the yield and tensile strengths were lower than those of the steels with more Mo and less Nb.

keyword : API X80, Linepipe steel, charpy impact test, separation

S-N fatigue behavior of cast 304 stainless steel was studied at 25, -50 and -196℃ and at a stress ratio of -1 in uniaxial and bending loading condition. It was found that the resistance to S-N fatigue was greatly improved with decreasing testing temperature. The normalized S-N fatigue curves by tensile strength at three different testing temperatures matched each other, suggesting that tensile strength determines the S-N fatigue resistance of cast 304 stainless steel at low temperatures. The effectsof different loading on the resistance to S-N fatigue of cast 304 stainless steel were quantified. The S-N fatigue curves at 25, -50 and -196℃ were described by using Basquin`s law the relationship between the S-N fatigue curve and the testing temperature was obtained by using a simple regression method.

keyword : cast 304 stainless steel, S-N fatigue, cryogenic temperatures

The effects of alloyed carbon on the pitting corrosion, the general corrosion, and the passivity behavior of Fe18Cr10Mn0.4NxC (x=0~0.38 wt%) alloys were investigated by various electrochemical methods and XPS analysis. The alloyed carbon increased the general corrosion resistance of the FeCrMnN matrix. Carbon enhanced the corrosion potential, reduced the metal dissolution rate, and accelerated the hydrogen evolution reaction rate in various acidic solutions. In addition, carbon promoted the pitting corrosion resistance of the matrix in a chloride solution. The alloyed carbon in the matrix increased the chromium content in the passive film, and thus the passive film became more protective.

keyword : metals, annealing, corrosion, SEM scanning electronmicros-copy, carbon

To reduce the heat released during intermetallic reaction, Ni-50at%Al powder compact has been previously annealed at several conditions before the reaction. The effects of the pre-annealing conditions on the reaction synthesis process have been investigated. Experimental results show that the heat released during the reaction synthesis decreased proportionally with increase of the pre-annealing temperature and duration time. The reaction duration period was significantly increased when the intermetallics were formed in the powder compact during the pre-annealing. This was attributed to the fact that the reaction occurred by solid-state diffusion between the un-reacted elemental atoms and that the NiAl3 phase formed predominantly during pre-annealing.

keyword : intermetallics, annealing, microstructure, thermal analysis, ration synthesis

In this study, the mechanisms of the three steps (the polymer deposition step, the polymer etching step and the Si etching step) that constitute the Bosch process were investigated. The effects of radicals and ions on each step were quantitatively analyzed by comparing the simulated aspect ratio dependency of the deposition or etch rate with the experimental results. In the polymer deposition step, fluorocarbon polymer is deposited by chemical reactions of CFx radicals, of which the reaction probability is 0.13. Although the polymer etching step and the Si etching step were conducted under the same conditions, the etching mechanisms of polymer and Si were found to be quite different. In the polymer etching step, both chemical etching and physical sputter-etching contribute to the polymer etching. Whereas, in the Si etching step, Si is chemically etched by F radicals, of which the reactivity is greatly increased by the bombardment of energetic ions.

keyword : semiconductors, bosch process, mechanism, computer simulation, reaction probability

The effect of the temperature on the resistivity of carbon black filled polymer matrix composites below and above percolation threshold (P(t)) was studied based on the electrical conduction mechanism. Temperature coefficient of resistance of the composites below percolation threshold changed from negative to positive at 0.195
keyword : composites, foaming, electrical properties, electrical resistivity

In this study, we have investigated the role of a metal oxide hole injection layer (HIL) between an Indium Tin Oxide (ITO) electrode and an organic hole transporting layer (HTL) in organic light emitting diodes (OLEDs). Nickel Oxide films were deposited at different deposition times of 0 to 60 seconds, thus leading to a thickness from 0 to 15 nm on ITO/glass substrates. To study the influence of NiO film thickness on the properties of OLEDs, the relationshipsbetween NiO/ITO morphology and surface properties have been studied by UV-visible spectroscopy measurements and AFM microscopy. The dependences of the I-V-L properties on the thickness of the NiO layers were examined. Comparing these with devices without an NiO buffer layer, turn-on voltage and luminance have been obviously improved by using the NiO buffer layer with a thickness smaller than 10 nm in OLEDs. Moreover, the efficiency of the device ITO/NiO (< 5 nm)/NPB/Alq3/ LiF/Al has increased two times at the same operation voltage (8 V). Insertion of a thin NiO layer between the ITO and HTL enhances the hole injection, which can increase the device efficiency and decrease the turn-on voltage, while also decreasing the interface roughness.

keyword : thin films, deposition, electrical properties, AFM, NiO