발간논문

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In the present study, the effect of variation in alloying elements on the carbide formation behavior during casting and homogenization treatment of M2 high speed steels was investigated. M2 high speed steels of various compositions were produced by vacuum induction melting. Contents of C, Cr, W, Mo, and V were varied from the basic composition of 0.8C, 0.3Si, 0.2Mn, 4.0Cr, 6.0W, 5.0Mo, and 2.0V in weight percent. Homogenization treatment at 1150℃ for 1.5 hr followed by furnace cooling was performed on the ingots. Area fraction and chemical compositions of eutectic carbide in as-cast and homogenized ingots were analyzed. Area fraction of eutectic carbide appeared to be higher in the ingots with higher contents of alloying elements the area fraction of eutectic carbide also appeared to be higher on the surface regions than in the center regions of ingots. As a result of the homogenization treatment, M2C carbide, which was the primary eutectic carbide in the as-cast ingots, decomposed into thermodynamically stable carbides, MC and M6C. The latter carbide was found to be the main one after homogenization. Fine carbides uniformly distributed in the matrix was found to be MC type carbide and coarsened by homogenization.

keyword : alloys, homogenization, decomposition, X-ray diffraction, carbide

Tensile tests are widely used for evaluating mechanical properties of materials including flow curves as well as Young`s modulus, yield strength, tensile strength, and yield point elongation. This research aims at analyzing the plastic flow behavior of high strength steels for automotive bodies using the finite element method in conjunction with the viscoplastic model considering the yield point elongation phenomenon. The plastic flow behavior of the high strength steel was successfully predicted, by considering an operating deformation mechanism, in terms of normalization dislocation density, and strain hardening and accumulative damage of high strength steel using the modified constitutive model. In addition, the finite element method is employed to track the properties of the high strength steel pertaining to the deformation histories in a skin pass mill process.

keyword : metals, deformation, mechanical properties, computer simulation, yield point elongation

Conventional rolling (symmetric) and differential speed rolling (DSR) were both applied to AA1050 sheets at various velocity ratios, from 1 to 2 between the top and bottom rolls. An electron backscatter diffraction (EBSD) technique was used to measure texture inhomogeneity through the thickness direction. After the annealing process, the annealing texture of the DSR processed sheets was different from that of conventionally rolled sheets. The velocity ratio between the top and bottom rolls affected the texture inhomogeneity and macroscopic plastic strain ratio of the AA1050 sheets. A prediction for the macroscopic plastic strain ratio of AA1050 sheets was carried out using a visco-plastic self-consistent (VPSC) polycrystal model. The strain ratio directionality that was predicted using the VPSC polycrystal model was in good agreement with experimental results.

keyword : DSR, FBSD, texture, plastic radio, polycrystal model

This study is concerned with tensile and Charpy impact properties of high-strength bainitic steels fabricated by controlled rolling process. Six kinds of steels were fabricated by varying finish rolling temperature, start cooling temperature, and cooling rate, and their microstructures and tensile and Charpy impact properties were investigated. Their effective grain sizes were also characterized by the electron backscatter diffraction analysis. The microstructures of the steels rolled in the single phase region were most similar to those of the steels rolled in the two phase region. The steels cooled from 700℃ were composed mainly of granular bainites, while those cooled from 600℃ contained a number of bainitic ferrites, which resulted in the decrease in ductility and upper shelf energy in spite of the increase in strength. In the steels cooling from 600℃, fine acicular ferrites were well formed when the cooling rate was slow, which led to the best combination of high ductility, high upper shelf energy, and low energy transition temperature according to the decrease in the overall effective grain size due to the presence of acicular ferrites having smaller effective grain size.

keyword : bainitic steels, metals, rolling, strength, tensile test

This study investigates the effects of porosity on the thermal stability and the thermal shock resistance of a porous nozzle used for blowing an inert gas. The samples of Al2O3-SiO2-ZrO2 system, which had the apparent porosity of 16~30% and bulk density of 2.6~3.2 g/cm3, were prepared by adding different graphite contents (5, 10, 20 wt%) as a pore-forming agent. The thermal shock test was conducted at ΔT=500, 1000, and 1400℃ also and the thermal stability was also carried out at 1550, 1600, and 1650℃ for 5 hrs. The specimen contained 10 wt% graphite had uniform pore size distribution, whereas the specimen with 20 wt% graphite showed non-uniform pore size distribution. As a result of thermal shock test, the specimen containing 10 wt% graphite appears to have higher mechanical strength than the other specimens (5, 20 wt% graphite). Both the 5 wt% and 20 wt% graphite specimens developed a non-uniform pore size distribution and cracks that were generated by intensive thermal stress.

keyword : porous materials, sintering, microstructure, scanning electron microscopy, SEM, durability

The present investigation has been performed on the mixing behavior and microstructural development during fabrication of Fe micro-nano powder feedstock for a micro-powder injection molding process. The mixing experiment using a screw type blender system was conducted to measure the variations of torque and temperature during mixing of Fe powder-binder feedstock with progressive powder loading for various nano-powder compositions up to 25%. It was found that the torque and the temperature required in the mixing of feedstock increased proportionally with increasing cumulative powder loading. Such an increment was larger in the feedstock containing higher content of nano-powder at the same powder loading condition. However, the maximum value was obtained at the nano-powder composition of not 25% but 10%. It was owing to the 'roller bearing effect' of agglomerate type nano-powder acting as lubricant during mixing, consequently leading to the rearrangement of micro-nano powder in the feedstock. It is concluded that the improvement of packing density by rearrangement of nano-powders into interstices of micro-powders is responsible for the maximum powder loading of about 71 vol.% in the nano-powder composition of 25%.

keyword : nanostructured materials, powder processing, microstructure, SEM, μ-PUM

Nanopowder of FeAl was synthesized by high energy ball milling. Using the pulsed current activated sintering method, a dense nanostuctured FeAl was consolidated within 2 minutes from mechanically synthesized powders of FeAl and horizontally milled powders of Fe+Al. The grain size and hardness of FeAl sintered from horizontally milled Fe+Al powders and high energy ball milled FeAl powder were 150 nm, 50 nm and 466 kg/mm2, 574 kg/mm2, respectively.

keyword : intermetallics, sintering, self-propagating synthesis, mechanical properties, X-ray diffraction

Interstitial free (IF) steel sheets were cold rolled by the cross-roll rolling mill in which the roll axes are tilted by ±7.5o away from the transverse direction of the rolled sample. After cross-roll rolling of IF steel sheets, the cold rolling and the recrystallization textures were distinguished from those observed after rolling in a normal rolling mill. The three-dimensional finite element method (FEM) simulation revealed that the operation of a large shear strain ε23 during cross-roll rolling leads to the formation of a distinct cold rolling texture. During recrystallization annealing, a pronounced change in texture components was not observed, which is attributed to the lack of either selective growth or oriented nucleation during the recrystallization process. Cold cross-roll rolling led to the formation of finer recrystallized grains in IF steel sheets.

keyword : rolling, texture, electron backscattering diffraction, EBSD, IF steel

When high-speed interrupted cutting is carried out for die and mold steels with high hardness, CBN tools manifested a significantly longer wear life than carbide, ceramic, or cermet tools in an experiment of face milling characteristics. In addition, it was also found that they secured a stable surface roughness within a range of 1.6 S~6.3 S, an acceptable range for precision machining for polished machining parts. And it makes them acceptable in the precision machining field, except in industries where very high machining accuracy is required. In the high hardness interrupted cutting, it was advantageous to perform a negaland treatment and a honning treatment on the tools` cutting edge to extend tool life and surface roughness. Also, severe crater development was found on the sloped face in CBN tools following high-speed machining. This caused the cutting edge to be weakened and damaged, and ultimately resulted in a shorter tool life. Finally, as a result of EDX mapping inspection, Cr component was detected evenly on the entire crater wear area, which can be included only in STD 11.

keyword : metals, machining, wear, scanning electron microscopy, SEM, interrupted culting

30 nm thick Ni layers were deposited on a glass substrate by e-beam evaporation. Subsequently, 30 nm or 60 nm α-Si:H layers were grown at low temperatures (<220℃) on the 30 nm Ni/Glass substrate by catalytic CVD (chemical vapor deposition). The sheet resistance, phase, microstructure, depth profile and surface roughness of the α-Si:H layers were examined using a four-point probe, HRXRD (high resolution Xray diffraction), Raman Spectroscopy, FE-SEM (field emission-scanning electron microscopy), TEM (transmission electron microscope) and AES depth profiler. The Ni layers reacted with Si to form NiSi layers with a low sheet resistance of 10Ω/□. The crystallinty of the α-Si:H layers on NiSi was up to 60% according to Raman spectroscopy. These results show that both nano-scale NiSi layers and crystalline Si layers can be formed simultaneously on a Ni deposited glass substrate using the proposed low temperature catalytic CVD process.

keyword : amorphous matrials, deposition, crystallization, transmission electronmicroscopy, TEM, thin films